The diffusion pump is the most common type of pump for use in high vacuum applications. If it is too low, backstreaming of oil from the mechanical pump into the diffusion pump occurs. Silicone based diffusion pump oil 1 gallon, same as dc705. The vacuum pump team consists of a vane vacuum pump and an oil diffusion pump. Some examples might be use of an oil sealed rotary vane pump the most common positive displacement pump backing a diffusion pump, or a dry scroll pump backing a turbomolecular pump. Educational guide to vacuum coating processing the oil diffusion pump often called the diff pump or dp is probably the most widely used highvacuum pump.
It required a low backing pressure and, at that time, was beyond the capabilities of any of my early forepumps. Operation, maintenance and troubleshooting of oil diffusion pumps oil diffusion pumps are still the most popular type of highvacuum pump because they. At this point, the vacuum diffusion pump takes over to create a. Performance of lion diffusion pump oil 11 corelationship between ultimate pressure temperature 1 pressure temperature relationship of lion diffusion pump oil a method. Oil diffusion pumps remain in popular use in the vacuum heat treating industry, possibly one of the few applications remaining for this type of high vacuum pump in the western world. The most common mechanical pumps are the single and multistage oil sealed mechanical pumps, such as the rotary vane pump shown in figure 1. This movie shows the function principles of the leybold oil diffusion pump dip. The oil jet with gas molecules hits the outer cooled shell of the oil diffusion pump. Hitachi hightechnologies will display s3700n at microscience 2006 in uk from june 27, the. Speed of oil diffusion pump do8001 with baffle and cod trap, pumping air 14 at the tate im d2, where mis the molecular weight. Agilent technologies diffusion pump operational manual. Vacuumbrand vario chemistry pumping unit pc 3001 variopro maximum nominal vacuum of 2 mbar rotary vane pump rvp.
The basic diffstak consists of a diffusion pump, a waterc ooled baffle, a highvacuum is olationvalve and a. By submitting this form, you consent that leybold gmbh will store and process your data according to our data privacy notice, i. Diffusion pumps are vapor jet pumps that work on the principle of momentum transfer. Every three months replace gas cylinders when below 500 psig. Edwards has long been a pioneer of vapour pumps and diffusion pump. Instead, an ancillary mechanical roughing pump or forepump, capable of a modest level of pumping, first brings the pressure inside the vacuum diffusion chamber down to about 103 torr. An oil diffusion pump is used to achieve higher vacuum lower pressure than is possible by use of positive displacement pumps alone.
Oil diffusion ejector vacuum pump pbl series ulvac. This dual stage rotary vane mechanical vacuum achieves lower ultimate pressure. Because of its simplicity, high performance and low initial cost, the diffusion pump is the primary industrial high vacuum pumping mechanism. According to dayto 2 the tate of speeds for hydrogen and air for a pump may be various, depend. The working fluid oil is heated in the boiler, vaporized and streams out of each stage of the jet stack at high speed. The basic diffstak consists of a diffusion pump, a waterc ooled baffle, a highvacuum is olationvalve and a roughing. Mt704 diffusion pump fluid is a single component fluid for high vacuums of 10e6 to 10e8 torr, untrapped or 10e10 to 10e11, trapped. When the rough pumps oil reaches the diffusion pumps boiler, it preferentially boils.
The fluid is then moved to another location and cooled. As discussed in our article covering the difference between hydrocarbon based and silicone based diffusion pump oil, we generally recommend our customers use silicone based diffusion pump oil. Lubrication, however, is not an easy job and is very dependent on the right selection. The pbl series are particularly wellsuited for the use as an intermediate pump between an oil rotary pump, a mechanical booster pump and oil diffusion pump. Many large scale industrial vacuum chambers are still diff pumped as they are very low maintenance, low cost and can scale up easily. Diffusion pumps differ from conventional mechanical pumps in that they use a high speed jet of fluid to direct gas molecules in the pump throat down to the bottom of the pump and out the exhaust, which is usually called the foreline. Santovac 5 polyphenyl ether lion s diffusion pump oil properties of pfeiffer p3 pumping fluid. Inland vacuums silicone diffusion pump oils invoil 702, 704, and 705 are durable fluids designed for a variety of high vacuum applications and for fast pumping large volumes of gas. The pumping effect of these pumps is created through the diffusion of gases into an oil vapor stream. High efficient vacuum pumps from leybold, best suited for industrial high vacuum applications. These vapor jet pumps are one of the oldest and most reliable ways to create a vacuum. If it is too high, backstreaming from the diffusion pump into the processing chamber occurs.
The fluid in a diffusion pump may have a vapor pressure 2 or 3 decades lower than a rough pumps fluid at the same temperature. In more critical applications, an opticallydense baffle is typically pro vided to deflect particles before they can reach the process stream. Your new online msds binder is a place for you to store the material safety data sheets you need to deploy. The main reasons for their continued use are their longevity the lack of other options.
Pdf 0 agilent varian ax65 diffusion pump service manual. Atomic energy commission reports available on this site. Product categories fomblin greases and fluids archive. Attainable ultimate pressures with oil diffusion pumps. Oil vapor diffusion pumps it wasnt that long ago when you could walk into any vacuum laboratory and find a vapor diffusion pump on every system. In all diffusion pumps, a small amount of backstreaming, movement of oil molecules into the vacuum chamber, occurs. Yet oil diffusion pumps require careful maintenance in order to sustain a high level of performance and maintain the integrity of the vacuum chamber. Safety data sheet reel efx diffusion fluid for use in the reel efx diffusion fogger df50 12. The dij series of diffusion pumps is a 5stage oil diffusion pump with an improved gas throughput and stable high pressure in the range of 103 mbar.
The oil is condensed and falls down to the boiler carrying with it the gas molecules. Diffusion pumps cannot discharge directly into the atmosphere, so a. A vacuum diffusion pump cannot begin its work with full atmospheric pressure inside the chamber. This is the foreline pressure the pressure through the rough pump. The vapor pressure and backstreaming rate of mt705 diffusion pump fluid are low enough that the use of traps or refrigeration may not be necessary for all ultrahigh and ultraclean vacuum applications. It performs well in tough, rugged applications and offers quick pumpdown, even after exposure to air at operating temperatures, although this is not recommended. The rotary vane pump removes these compressed gas molecules at the exhaust port of the diffusion pump. The oil diffusion pump consists of a pump body, boiler heater and 3stage fractionating jet stack assembly. It is very reliable and longlived, although when misused it can create a great deal of contamination in the processing chamber. The turbo pump still cannot compete price and size wise with the diffusion pump. Dec 02, 2019 gee, it kinda stops at about 1950 and 108 torr. Silicone based diffusion pump oil 500 cc, same as dc704.
We routinely pulled to 1015 torr using diffusion pumps on tubes in an oven at 850 degrees in the glass room at datagraphics. The measurements of the jet breakdown pressure of an oil diffusion pump have been taken in respect of the heat input, and those of the pumping speeds have been taken both in relation to heat input and forepressure, both for air and for hydrogen. To achieve a higher vacuum, other techniques must then be used, typically in series usually following an initial fast pump down with a positive displacement pump. Vacuumbrand highvacuum pumping unit hp 40 b2rz 6 maximum nominal vacuum of 1. Chemstar dry oil free deep vacuum download our price list. Note that an image format with 1m pixels is generally used for the electronic file.
The mk2 series of diffstaks are compact highperformance diffusion pumps which provide exceptionally clean pumping without the use of extra traps or baffles or the need for liquid nitrogen cooling. Oil rotary vacuum pump vd series is a directdrive oil rotary pump with high efficiency ie3 multivoltage motor fully developed by ulvac. Every month clean the splitsplitless inlet vent line trap. These components are essential for preventing the return flow of oil in the pump. Ecological information oil based fluid will be inherently biodegradable in water under aerobic conditions, and will be ultimately biodegrades by microorganisms although the biodegrability of oil based fluid will necessarily be limited by its. The oil booster pump ob has one or more fourstage nozzle systems and one or more jet stages. Ideal vacuum vacuum pump user manuals pdf downloads. Oil diffusion pumps 3000 50000 l x s1 oils, baffles, accessories. These oils were useful because they remained in the pump indefinitely and allowed lower.
Bridge 4 oil diffusion pump one of 3,612 items in the series. Other companies are charging thousands of dollars to set up accounts and give you access to their msds online database. Check the foreline pump oil level and diffusion pump fluid. Vapor diffusion pumps were first conceived about 191516, and used mercury as the pumping fluid. Oil diffusion pumps most innovative design for best performance and efficiency. Maintenance and troubleshooting of oil diffusion pumps. The weight is 25 kg for the diffusion pump mainframe, 26 kg for the standard turbo pump mainframe, and 29 kg for the performance turbo pump mainframe. Prevent further leakage or spillage if safe to do so.
When the oil view diffusion pump oil selection online becomes hot enough to vaporize, the oil vapors rise up the center of the pump and exit the nozzles at a downward angle. Since the chamber itself has no moving parts aside from the oil droplets, a vacuum. The larger capacity pumps pbl06 pbl20 have the heaters directly immersed in the operating fluid for maximum thermal efficiency. The working principle of oil diffusion pump is similar to that of water vapor injection pump, both of which carry gas by high speed steam jet to achieve the purpose of air extraction. The features that make the diffusion pump attractive for high and ultrahigh vacuum use are its high pumping speed for all gases and low cost per unit pumping speed when compared with other types of pump used in the same vacuum range.
Using silicone based oil, there is little or no maintenance required, just several things. The oil diffusion pumps are vibrationfree, reliable, and less expensive, while they may introduce contamination because of oil vapor. Maintenance and troubleshooting of oil diffusion pumps agilent. After it has been verified that the roughing pump is operating correctly begin warming the diffusion pump users manual for specifics and connect it to the system. These nozzles are in a ring and form a curtain or skirt of vapor that extends from the nozzles to the pump wall. For pump operation, the boiling point of the oil is not particularly important, but the thermal breakdown temperature may be.
We meet customers needs with various lineup including 4 to 52 inch for oil diffusion pump and 2 to 20 inch for oil diffusion ejector pump. The oil diffusion ejector pump consists of a pump body, heater and 3stage jet stack assembly. Stainless steel is used for the pump bodies of model pbl02 and pbl04 in order to minimize outgassing of the pumps, eliminate corrosion and to ensure a long operating lifetime of the pump. The diffusion pump uses the vapor of a boiling fluid to capture air molecules. Diffusion pump maintenance guide diffusion pump oil by. When your process requires a pressure below that of a mechanical pump or mechanical pump and roots pump combination a. The heating zone with constant temperatures is at the middle part of the quartz tube, and at the both ends of tubes far from the heating zone are condensing zones. Mt705 diffusion pump fluid is a colorless to light straw, a single component for ultrahigh vacua in the range of 10e9 to 10e10 torr untrapped and 10e11 torr trapped. The oil and the jets are examined frequently and the performance of the pump monitored apiezon. This cyclic process creates the pumping action of an oil diffusion pump. Oil diffusion pumps are still the most popular type of highvacuum pump because they are relatively inexpensive, highly reliable and very durable. Busch r 5 ra 0400 0630 c oil lubricated rotary vane vacuum pumps.
This article will explain practical steps that can be taken to ensure optimal performance of. Use and maintenance of oil diffusion pump vacuum pump. Until the high vacuum valve 4 opens, both diffusion pump and pump fluid are preserved. High throughput gives high pumping speeds at high pressures, earlier cross over from backing pump set to the diffusion pump, thus reducing pump down time to process pressure. Edwardss range of high throughput diffusion pumps have many advantages in industrial applications. General applications and accessories for oil diffusion pumps. Please note that in these tips, we will use the terms oil and fluid interchangably. Agilent diffusion pumps offer high pumping speeds, high throughput, high tolerance forepressure, excellent backstreaming characteristics, low ultimate pressure, and longterm reliability. When designing a system with diffusion pumps it must be noted that the angle valve and the water baffle reduce the pumping speed of a diffusion pump by about 40%.
In practice, to reduce specimen contamination, a diffusion pump oil of low vapor pressure should be employed. Although its use has been mainly associated within the highvacuum range down to 10. Before venting the vacuum chamber the forevacuum valve 2and the high vacuum valve 4must be closed, whereby the diffusion pump remains in the ready status. Silicone based diffusion pump oil 100 cc, same as dc705. Even as turbomolecular vacuum pumps have displaced most small laboratory sized oil diffusion pumps these days because of perceived ease of use and cleanliness, most high vacuum heat treating furnaces still rely on a large oil diffusion pumps to generate the pressures below about 103 torr needed for many metal conditioning processes. Thus, these components are evacuated generally by a diffusion pump. If a user desires an oilfree environment, a turbo molecular. The diffusion pump should not be connected to the rest of the vacuum system until after the roughing pump had had a chance to thoroughly evacuate the vacuum system. Figure 1 shows the cross section of a typical oil diffusion pump. Information about dow corning diffusion pump fluid dow.
Typical applications n vacuum coating n metallurgy n. By using turbomolecular pump tmp as standard, the new s3700n reduces electricity consumption by about 34% and foot print by about 27% 2 compared to conventional model which adopts the oil diffusion pump. Oil diffusion pumps are still a widely used type of high vacuum pump. Oil diffusion pump ulkpflpbl series pbl series oil. On the pumping speed of oil diffusion pumps springerlink. The ulvac diffusion pumps have been designed for outstanding performance and extremely low running costs. The list of pump failure conditions mentioned above is neither exhaustive nor are the conditions mutually exclusive. Oil diffusion ejector pumpy pbl series ulvacs oil diffusion pump has been used for many high vacuum equipments. The difference is that the diffusion pump works in the high vacuum area, and its working pressure range is 102 106pa.
The attached foreline roughing pump weighs an additional 11 kg standard pump. Jan 06, 2015 its purpose is to achieve higher vacuum. New scanning electron microscope model s3700n is released. Vapor pressure as figure 1 shows, dow corning 705 diffusion pump fluid has extremely low vapor pressure. Leybold may also forward your data to its distributors and partners in order to process your enquiry. Essential oil use chart a b c d e,f g h i,j,k l,m n,o p,q r s t u,v,w x,y,z blends and other products are by doterra. The oildiffusion pumps can reach a vacuum of 500 ls. The pumping speed ranges from 6,000 to 18,000 ls and has a operating pressure range from 101 to 104 mbar. Leybonol lvo 521 is our new highpurity, highquality silicone oil solution for your diffusion pump. R 5 ra 0400 0630 c busch vacuum solutions united states. Depending on the type of diffusion pump oil you use, maintenance can be relatively simple to very time consuming. Vacuum system the inside of the electron optical system and the specimen chamber must be kept at a high vacuum of 103 to 104 pa. Old comment, but even in 2011 the oil diffusion pump isnt going anywhere.